Organic structures from spectra / L.D. Field

Contents

preface
list of tables
list of figures

1. INTRODUCTION
1.1 General principle of absorption spectroscopy
1.2 Chromophores
1.3 Connectivity, etc

2. ULTRAVIOLENT (UV) SPECTROSCOPY
2.1 Basic instrument
2.2 The nature of ultraviolent spectroscopy
2.3 Quantitative aspects of ultraviolent spectroscopy, etc

3. INFRARED (IR) SPECTROSCOPY
3.1 Absorption range and the nature of IR absorption
3.2 Experimental aspects of Infrared spectroscopy
3.3 General features of infrared spectra, etc

4. MASS SPECTROMETRY
4.1 Ionisation processes
4.2 Instrument
4.3 Mass spectral data, etc

5. NUCLEAR MAGNETIC RESONANCE (NMR) SPECTRSCOPY
5.1 The physics of nuclear spins and NMR instruments
5.2 Continuous wave (WV0 NMR spectroscopy
5.3 Fourier-transform (FT) NMR spectroscopy, etc

6. 13C NMR SPECTROSCOPY
6.1 Coupling and Decoupling in 13C NMR spectra
6.2 Determine 13C signal Multiplicity using Dept.
6.3 Shielding and characteristics chemical shifts in 23 C NMR Spectra, etc

7. 2-DIMENSIONAL NMR SPECTROSCOPY
7.1 cosy (Correlational spectroscopy)
7.2 The HSQC (Heteronuclear single quantum)
7.3 HMBC (Heteronuclear multiple bond correlation), etc

8. MISCELLANEOUS TOPICS
8.1 Solvents for NMR spectroscopy
8.2 Solvent induced shifts
8.3 Dynamic processes in NMR - The NMR time-scale, etc

9. DETERMING THE STRUCTURE OF ORGANIC COMPOUNDS FROM SPECTRA
9.1 solving problems
9.2 worked examples

10. PROBLEMS
10.1 Spectroscopic identification of organic compounds
10.2 The analysis of mixtures
10.3 problems in 2-dimensional NMR, etc

Includes subject index : p. 493-495